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  5. Characterization of Terpenoids from the Ambrosia Beetle Symbiont and Laurel Wilt Pathogen Harringtonia lauricola.

Characterization of Terpenoids from the Ambrosia Beetle Symbiont and Laurel Wilt Pathogen Harringtonia lauricola.

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Resource type
Journal article
Creator (person)
Zhu, Zhiqiang
ORCIDORCID logo
Yang, Chenjie
Keyhani, Nemat O.
ORCIDORCID logo
Liu, Sen
Pu, Huili
Jia, Peisong
Wu, Dongmei
Stevenson, Philip C.
ORCIDORCID logo
Fernández-Grandon, G. Mandela
ORCIDORCID logo
Pan, Jieming
Chen, Yuxi
Guan, Xiayu
Qiu, Junzhi
ORCIDORCID logo
Date published
December 7, 2023
Abstract
Little is known concerning terpenoids produced by members of the fungal order Ophiostomales, with the member Harringtonia lauricola having the unique lifestyle of being a beetle symbiont but potentially devastating tree pathogen. Nine known terpenoids, including six labdane diterpenoids (1–6) and three hopane triterpenes (7–9), were isolated from H. lauricola ethyl acetate (EtOAc) extracts for the first time. All compounds were tested for various in vitro bioactivities. Six compounds, 2, 4, 5, 6, 7, and 9, are described functionally. Compounds 2, 4, 5, and 9 expressed potent antiproliferative activity against the MCF-7, HepG2 and A549 cancer cell lines, with half-maximal inhibitory concentrations (IC50s) ~12.54–26.06 μM. Antimicrobial activity bioassays revealed that compounds 4, 5, and 9 exhibited substantial effects against Gram-negative bacteria (Escherichia coli and Ralstonia solanacearum) with minimum inhibitory concentration (MIC) values between 3.13 and 12.50 μg/mL. Little activity was seen towards Gram-positive bacteria for any of the compounds, whereas compounds 2, 4, 7, and 9 expressed antifungal activities (Fusarium oxysporum) with MIC values ranging from 6.25 to 25.00 μg/mL. Compounds 4, 5, and 9 also displayed free radical scavenging abilities towards 2,2-diphenyl-1-picrylhydrazyl (DPPH) and superoxide (O2−), with IC50 values of compounds 2, 4, and 6 ~3.45–14.04 μg/mL and 22.87–53.31 μg/mL towards DPPH and O2−, respectively. These data provide an insight into the biopharmaceutical potential of terpenoids from this group of fungal insect symbionts and plant pathogens.
Project(s)
Priority 2: Trait Diversity and Function
Funder
Funder nameAwards
National Natural Science Foundation of China, China
No. 32270029 - No. U1803232 - No. 31670026
National Key Research and Development Program of China, China
No. 2017YFE0122000
Social Service Team Support Program Project, China
11899170165
Fujian Agriculture and Forestry University, China
Science and Technology Innovation Special Fund (no. KFB23084)
Fujian Provincial Major Science and Technology Project, China
2022NZ029017
Fujian Provincial Department of Science and Technology, China
Key Project (no. 2020N5005)
Young and Middle-aged Teacher Education Research Project of Fujian Province
JAT210075
National Science Foundation, United States
IOS-2241029
U.S. Department of Agriculture, United States
NIFA award 2019-05150
Journal title
Journal of Fungi
Volume
9
Issue
12
Article number
1175
Publisher
MDPI AG
Place of publication
Basel, Switzerland
eISSN
2309-608X
Date accepted
December 5, 2023
Official URL
https://doi.org/10.3390/jof9121175
Related URL
https://www.mdpi.com/2309-608X/9/12/1175
Rights statement
In Copyright
Licence
https://creativecommons.org/licenses/by/4.0/
DOI
10.3390/jof9121175
Keywords
Secondary metabolite
Antiproliferative
Harringtonia lauricola
Antimicrobial
Laurel wilt
Xyleborus glabratus
Free radical scavenging
Ophiostomales
Terpenoid
Additional information
IF = 5.724 (2022-2023)
Managed by the British Library and supported by the AHRC

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